Instrumental Analysis Skoog Solution Manual Ch 16
CHEM.3440 Instrumental Analysis Home Page Instrumental Analysis CHEM.3440 Fall 2006 Offering Lecturer: Dan Thomas MACN 120/121/128 x53961 SCIE 1316 x52388 Lab Coordinator: Julie De Merchant SCIE 3113A x54861 Lab Demonstrator: Christa Brosseau MACN 135 Lectures: Mon, Wed, Fri 8:30 - 9:20 A.M. In MACK 233 Laboratory: Thurs. 2:30 - 5:20 P.M. In SCIE 3105, Thurs.
7:00 - 9:50 P.M., Fri. 2:30 - 5:20 P.M. Note: Lecture is cancelled on Friday, September 29 as I will be away that day. Evaluation Textbook Assignments: 10% Spreadsheet Assignments: 10% Laboratory: 30% Mid-Term Exam: 20% (Date of exam is Tuesday, October 24, 7:00 - 9:00 P.M. It is to be held in MACK 233.) Final Exam: 30% (Date of exam is Saturday, December 9 from 11:30 A.M.
To 1:30 P.M.) Exam location is Crop Science 116/117. Textbook: 'Principles of Instrumental Analysis', Skoog, Holler, and Nieman (Thomson Learning Inc.) You will need regular access to this book as you will be asked to read numerous chapters and the homework assignments are from the problems in the text.
The textbook and several other texts that would be sueful for study are on reserve in the library. Lecture Topics. Statistical Methods for Analytical Chemistry. Analog Electronics.
Elementary Circuit Analysis. Signal Modification by Filters. Operational Amplifiers. Digital Electronics.
Spectrometry. UV/Visible Spectrometry. Light sources, detectors, spectrometers. Analytical experiments. Luminescence Spectrometry.
Fluorescence and Phosphorescence. Infrared Spectrometry. Fourier Transform, FTIR. Light sources, detectors, spectrometers. Raman Spectrometry.
Comparison with IR. Mass Spectrometry.
Molecular analytes. Sources, Mass Analyzers, and Detectors. X-ray Fluorescence Spectrometry. Sources, Spectrometers, Detectors. Thermal Methods.
TGA, DTA, DSC. Radiochemical Methods. Neutron Activation. Lecture Notes The lecture notes can be downloaded from here. They are available in pdf format. Section 1 Section 2 Section 3 Section 4 Section 5 Section 6 Section 7 Section 8 Section 9 Section 10 Section 11 Section 12 Section 13 Section 14 Section 15.
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Solutions Due Date Chapter 1 & Chapter 2 2-1, 2-3, 2-7, 2-14, 2-15, 2-18, 2-19 Note error in question 2-18(c). Capacitance should be 0.033. Also, answers in back of book are wrong for many of the answers for this question. Also, you will need to use some equations from the book. For equation 2-49, the numerator should the number 1, not the variable I. Also, they messed up the phase calculations in the impedance in an RC circuit.
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To be done correctly, it should really be done with complex arithmetic. They throw out all that extra information and then put it back in incorrectly.
The phase angle calculation (equations 2-43 and 2-45) should have a minus sign in front of the arctan function. This is because the reactance is a negative quantity.
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